Abstract: Easy preparation of iron oxide nanoparticles [5- and 11-nm maghemite (γ-Fe 2O 3) and 19-nm magnetite (Fe 3O 4)] by thermal decomposition of Fe(CO) 5 in the presence of residual oxygen of the system and by consecutive aeration were investigated by TEM/HRTEM. The superparamagnetic 5- and 11-nm γ-Fe 2O 3 and ferrimagnetic 19-nm Fe 3O 4 particles were easily prepared by thermal decomposition of Fe(CO) 5 in the presence of residual oxygen of the system and by consecutive aeration, and their magnetic properties were investigated.

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